HOTLINE HEATING Huffman 709233.pdfFRIEDMAN & BRUYA, INC.
ENVIRONMENTAL CHEMISTS
James E. Bruya, Ph.D.
Yelena Aravkina, M.S.
Michael Erdahl, B.S.
Arina Podnozova, B.S.
Eric Young, B.S.
September 20, 2017
Gary VanCleave
Hotline Heating
PO Box 46232
Seattle, WA 98146
Dear Mr VanCleave:
3012 16th Avenue West
Seattle, WA 98119-2029
(206) 285-8282
fbi@isomedia.com
www.friedmanandbruya.com
Included are the results from the testing of material submitted on September 14, 2017
from the Huffman, F&BI 709233 project. There are 3 pages included in this report.
Any samples that may remain are currently scheduled for disposal in 30 days. If you
would like us to return your samples or arrange for long term storage at our offices,
please contact us as soon as possible.
We appreciate this opportunity to be of service to you and hope you will call if you
should have any questions.
Sincerely,
FRIEDMAN & BRUYA, INC.
Michael Erdahl
Project Manager
Enclosures
NAA0920R.DOC
FRIEDMAN & BRUYA, INC.
ENVIRONMENTAL CHEMISTS
Date of Report:
09/20/17
Date Received:
09/14/17
Project: Huffinan, F&BI 709233
Date Extracted:
09/15/17
Date Analyzed:
09/15/17
RESULTS FROM THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL PETROLEUM HYDROCARBONS AS DIESEL
USING METHOD NWTPH-Dx
Extended to Include Motor Oil Range Compounds
Results Reported on a Dry Weight Basis
Results Reported as mg/kg (ppm)
Sample ID
Laboratory ID
Soil Sample No. 1
709233-01
Method Blank
07-2031 MB
Surrogate
Diesel Extended (% Recovery)
(C10-C36) (Limit 56-165)
22,000 99
<50 95
I
FRIEDMAN & BRUYA, INC.
ENVIRONMENTAL CHEMISTS
Date of Report: 09/20/17
Date Received: 09/14/17
Project: Huffinan, F&BI 709233
QUALITY ASSURANCE RESULTS FROM THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL PETROLEUM HYDROCARBONS AS
DIESEL EXTENDED USING METHOD NWTPH-Dx
Laboratory Code: 709234-01 (Matrix Spike)
Sample
Percent Percent
Reporting
Spike
Result
Recovery Recovery Acceptance RPD
Analyte
Units
Level (Wet
Wt)
MS MSD Criteria (Limit 20)
Diesel Extended
mg/kg (ppm)
5,000
<50
92 92 63-146 0
Laboratory Code:
Laboratory Control Sample
Percent
Reporting
Spike
Recovery
Acceptance
Analyte
Units
Level
LCS
Criteria
Diesel Extended
mg/kg (ppm)
5,000
90
79-144
2
FRIEDMAN & BRUYA, INC.
ENVIRONMENTAL CHEMISTS
Data Oualifiers & Definitions
a - The analyte was detected at a level less than five times the reporting limit. The RPD results may not
provide reliable information on the variability of the analysis.
b - The analyte was spiked at a level that was less than five times that present in the sample. Matrix
spike recoveries may not be meaningful.
ca - The calibration results for the analyte were outside of acceptance criteria. The value reported is an
estimate.
c - The presence of the analyte may be due to carryover from previous sample injections.
cf - The sample was centrifuged prior to analysis.
d - The sample was diluted. Detection limits were raised and surrogate recoveries may not be
meaningful.
dv - Insufficient sample volume was available to achieve normal reporting limits.
f - The sample was laboratory filtered prior to analysis.
fb - The analyte was detected in the method blank.
fc - The compound is a common laboratory and field contaminant.
hr - The sample and duplicate were reextracted and reanalyzed. RPD results were still outside of control
limits. Variability is attributed to sample inhomogeneity.
hs - Headspace was present in the container used for analysis.
ht — The analysis was performed outside the method or client -specified holding time requirement.
ip - Recovery fell outside of control limits. Compounds in the sample matrix interfered with the
quantitation of the analyte.
j - The analyte concentration is reported below the lowest calibration standard. The value reported is an
estimate.
J - The internal standard associated with the analyte is out of control limits. The reported concentration
is an estimate.
jl - The laboratory control sample(s) percent recovery and/or RPD were out of control limits. The
reported concentration should be considered an estimate.
s - The surrogate associated with the analyte is out of control limits. The reported concentration should
to The
an estimate.
lc - The presence of the analyte is likely due to laboratory contamination.
L - The reported concentration was generated from a library search.
nm - The analyte was not detected in one or more of the duplicate analyses. Therefore, calculation of the
RPD is not applicable.
pc - The sample was received with incorrect preservation or in a container not approved by the method.
The value reported should be considered an estimate.
ve - The analyte response exceeded the valid instrument calibration range. The value reported is an
estimate.
vo - The value reported fell outside the control limits established for this analyte.
x - The sample chromatographic pattern does not resemble the fuel standard used for quantitation.
3
' 7— 3 7 SAMPLE CHAIN OF CUSTODY
Report To d� f--' G SAMPLERS (signature)
Company -�- ` ' L PROJECT NAME
Address
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PO #
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Page #
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TURNAROUN I) TIME
0 Standard Turnaround
0 RUSH
Rush charges authorized by:
SAMPLE DISPOSAL
0 Dispose after 30 days
0 Archive Samples
0 Other
ANALYSES
REQUESTED
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Lab ID
Date
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Time
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Sample
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Friedman & .Bruya, TAc.
301216t" Avenue West
Seattle, WA 98119-2029
Ph. (206) 285-8282
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Relinaauished b't � �. �., � .. ...____.._............... _._._..........._......_._
Received by
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